Win against Cyrus (Team Galactic boss ) He will give you a masterball.
Follow his instructions.
Buy a bunch of ultra balls (30 should be enough) and a couple of quick balls.
Go to Mt. Coronet.
Climb to the top to Spear Pillar. Beware wild Pokémon such as Bronzong.
Defeat Galactic Commanders Mars and Jupiter in a Double Battle with your rival.
Watch the cut scene, if you want.
Defeat Cyrus for the second time.
Save your game before you talk to Palkia. This way, if you fail to catch it, you can start over.
When catching, do NOT use a Masterball. The catch rate of this Pokémon is high for legendary Pokémon. Instead weaken with an attack and then chuck quick balls. Because quick balls lose their effectiveness after 5 turns, switch to ultra balls. You probably won't even need the ultra balls if it takes only one hit to get Palkia down to red.
Run north to get an Orb that powers up Palkia's attacks.
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