Get a Sea Incense.
The Sea Incense is located in Mt. Pyre, which you have to reach the top floor (after you defeat Hex Maniac Valerie) and fall through the holes in the floor to reach it. Once you get to the top floor, drop down to the hole to fifth floor. There will be a Lax Incense on this floor. You may pick it up, but it is not needed to obtain Azurill. Fall through the lower of the 2 holes. This will allow you to get the Sea Incense on the next floor.
Obtain two Marill (one male one female).
Marill are located in multiple places. While surfing, they are located at routes 102, 111, 114, 117, Petalburg City, and the Safari Zone. While in tall grass, they are located at routes 104, 112, 117, and 120.
Go to the daycare.
The daycare is located on route 117, between Verdanturf and Mauville.
Place the Sea Incense on one of the Marill.
To give a Pokémon an item, go to your bag, select the item, and give to a Marill.
Place them into the daycare.
When you place one in the daycare, the woman will ask to deposit another one. Hit yes, and select the other Marill.
Wait.
You will have to wait a bit (between 2-4 minutes maybe) for an egg to be made. You can't stand still. You have to move your character around.
Obtain an egg.
The old man should turn around and offer you an egg. You can only accept if you have an empty slot in your party.
Hatch the egg.
Hatching the egg will take some time, but all you have to do is walk around until it hatches.
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